Ultra-high magnetic field NMR spectrometers operating at proton frequencies approaching and exceeding 1.2 GHz are opening new opportunities for biomol…

Precise 13C NMR chemical shifts were measured for a set of reference compounds on five solid-state NMR instruments to evaluate reproducibility across …

Solid-state NMR faces limitations for liquid sample analysis due to the incompatibility with the magic angle spinning (MAS) method used for averaging …

A method to obtain magnetic dipole-dipole coupling information for nuclei exhibiting ultra-wideline NMR spectra in disordered solids is presented. Thi…

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Layered boron nitride (BN) is a two-dimensional (2D) insulator that exhibits several polytypes, which differ in the stacking sequence of adjacent atom…

137Ba nuclear quadrupole interactions (NQI) are measured in zero field using nuclear quadrupole resonance (NQR) for a series of compounds, (BaBr2.2H2O…

This paper describes the first known detection of cobaltite (CoAsS) by 75As NQR spectroscopy. The 75As resonance was observed from a natural cobaltite…

Understanding Lithium-ion conduction mechanisms is key to develop new solid-state electrolytes. However, Li-ion dynamics in glassy electrolytes are in…

Magic-angle spinning (MAS) NMR is predicated on the requirement that the rotor spin at the magic angle, yet in current practice, the effective rotor a…

Owing to their high stability, Zr-based Metal-Organic Frameworks (MOFs) named UiO-66 are promising materials for CO2 adsorption. Nevertheless, their r…

Three-dimensional (3D) spectra are essential for resonance assignment of complex biomolecules. Here we present a CCC spectrum that correlates the thre…

Manganese oxides (MnOx) represent an important and versatile class of electrode materials for electrochemical energy-storage technologies, particularl…

Nuclear magnetic resonance (NMR) measurements of the hyperfine parameters (quadrupolar, shifts) at the metal and boron sites are reported from an isom…

The nuclear quadrupole coupling constant at the boron site, in a series of sixteen isomorphous metal hexaborides with the CaB6 structure, is shown to …

17O NMR spectroscopy is emerging as a powerful probe of the chemistry of CO2 capture and storage materials. However, the technique is currently underu…

The characterization of hydrated polysaccharide assemblies by solid-state NMR (ssNMR) remains challenging because hydration modifies proton networks, …

Solid-state NMR (ssNMR) relies on sophisticated pulse sequences to obtain information on spin systems in solids or semi-solids. Analytical derivations…

Trier is the oldest City in Germany with many relicts of the Roman empire. One of them is the burial chamber at Reichertsberg. Since its discovery in …

Ultrahigh-field solid-state NMR in the GHz frequency range has opened new frontiers for probing complex, heterogeneous biological systems with unprece…

The description of a 3D printed magic angle spinning (MAS) stator capable of stably spinning single powdered solid samples in 4 mm diameter printed ro…

A fundamental understanding of lithium-ion (Li+) interactions and ion-transport mechanisms in electrolytes is essential for the development of high-pe…

Quadrupole central transition (QCT) NMR has recently been shown to be an effective way of obtaining high spectral resolution for half-integer quadrupo…

A simple method for computing J couplings from first principles is proposed, implemented, and tested. In this approach the coupling, which is just the…

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Recent advancements in solid-state NMR (ssNMR) techniques have facilitated the structural analysis of various biomaterials formed by carbohydrates, proteins, lipids, and other biomolecules. These inve...

We review solid-state NMR of magnetically oriented microcrystals. Three-dimensional alignment makes experiments virtually equivalent to single-crystal…